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Extra resources for Characterization of Metal and Polymer Surfaces. Volume 1: Metal Surfaces

Sample text

27. S. V . K r i s h n a s w a m y 1049 (1974). 28. 29. E . W . M u l l e r , J. M i c r o s c o p y ( O x f o r d ) , 1 0 0 , 1 2 1 ( 1 9 7 4 ) . E . W . M u l l e r , P r o c . S e c o n d I n t e r n . C o n f . on S o l i d S u r f a c e s , K y o t o , J a p a n , J a p a n J. A p p l . P h y s . , S u p p l . 2 , p a r t 2 , 1 (1974). W . P.

Muller and S. V . PUM P F i g . 7. T h e 1 9 7 5 h i g h r e s o l u t i o n , e n e r g y f o c u s e d ToF a t o m - p r o b e . Top v i e w shows the microscope chamber equipped with a s w i n g - a w a y c h a n n e l p l a t e - s c r e e n a s s e m b l y , w h i l e t h e side view shows a previously used channel plate-screen with a probe hole. C O d e s o r b e d from t u n g s t e n , V ^ c w a s g r a d u a l l y r a i s e d from 1 9 , 4 0 0 to 2 1 , 0 0 0 V to m a i n t a i n an a b o u t c o n s t a n t e v a p o r a t i o n r a t e w h i l e the tip radius increased.

In s h o r t , t h e r e s e e m s t o b e no way to assure the basic requirement of a precise time-of-flight a t o m - p r o b e , w h i c h is t o h a v e all p a r t i c l e s e n t e r i n g the d r i f t p a t h with a well defined energy. T h e s o l u t i o n o f t h i s p r o b l e m is the c o m p e n s a t i o n of e n e r g y d e f i c i t s b y ion o p t i c a l m e a n s . W e first u s e d the e n e r g y d i s c r i m i n ­ a t i o n o f a 90° c y l i n d r i c a l o r s p h e r i c a l e l e c t r o s t a t i c s e c t o r field and i n c l i n e d t h e d e t e c t o r f r o n t p l a t e w i t h r e s p e c t t o t h e o p t i c a l 2 2 89 t r a v e l e d a a x i s in s u c h a w a y t h a t t h e m o r e d e f l e c t e d s l o w5 e r6 ions shorter path than the more energetic s p e c i e s .

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