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1%–10%) Major (>10%) X-ray diffraction No No No Yes Yes Nuclear magnetic resonance No No Yes Yes Yes X-ray fluorescence No No Yes Yes Yes Infrared spectroscopy No No Yes Yes Yes Raman spectroscopy No No Yes Yes Yes UV/VIS spectrometry No No Yes Yes Yes Colorimetry No Yes Yes Yes No Molecular fluorescence spectrometry Atomic absorption spectrometry No Yes Yes Yes Yes Yes Yes Yes Yes No Atomic emission spectrometry Yes Yes Yes Yes Yes Atomic fluorescence spectrometry ICP-mass spectrometry Yes Yes Yes No No Yes Yes Yes Yes No Organic mass spectrometry Yes Yes Yes Yes Yes GC-MS Yes Yes Yes Yes Yes LC-MS Yes Yes Yes Yes Yes Potentiometry No Yes Yes Yes Yes Voltammetry No Yes Yes Yes Yes Gas chromatography May be Yes Yes Yes Yes High-performance liquid chromatography Ion chromatography May be Yes Yes Yes Yes May be Yes Yes Yes Yes Capillary electrophoresis No Yes Yes Yes Yes Thermal analysis Yes No No Yes Yes Note: The destructive nature of the instrumental method is characterized.

4 Sampling of a segregated material with a problematic component like gold. , A Manual for the Chemical Analysis of Metals, ASTM International, West Conshohocken, PA, 1996. With permission. ) (the white area). If the rock is crushed to Size I, the gold particles have not been liberated from the quartz; some pieces have gold flecks and many large pieces are pure quartz. At this size, it is difficult to remove a sample of the rock pieces and expect it to be representative. If the rock is crushed to a smaller size, Size II, it is evident that a representative small sample can be obtained.

There are many analytical procedures and methods that have been developed and published for a wide variety of analytes in many different matrices. These methods may be found in the chemical literature; in journals such as Analytical Chemistry, The Analyst, Analytical and Bioanalytical Chemistry (formerly Fresenius’ Journal of Analytical Chemistry), and Talanta; and in journals Concepts of Instrumental Analytical Chemistry 13 that focus on specific analytical techniques, such as Applied Spectroscopy, Journal of Separation Science (formerly Journal of High Resolution Chromatography), Journal of the American Society for Mass Spectrometry, and Thermochimica Acta.

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