By John Edward Cantle (Eds.)
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Additional info for Atomic Absorption Spectrometry
In the author's laboratory, asbestos lined cupboards coated with chlorinated rubber paint have given many years of trouble-free service; both ducts and walls are washed down at intervals. A further point to note here is that many laboratory fume exhaust systems use common ducts to a number of cupboards, and the mixing of exhausts from fuming perchloric acid and, say, the evaporation of alcohols in a separate cupboard could lead to an unexpected reaction in the ducts. Having stressed some of the precautions to be taken, it is perhaps necessary to list the advantages of using perchloric acid, with particular reference to its use in wet oxidation procedure.
G. Jones and A. Walsh, Spectrochim. Acta, 16 (1960)249. J. V. Sullivan and A. Waish, Spectrochim. Acta, 21 (1965)721. B. J. Russel and A. Walsh, Spectrochim. Acta, 15 (1959)883. C. Candler, Atomic Spectra, D. , 1964. H. Kahn, At. Absorpt. , 7 (1968)40. A. Menzies, Anal. , 32 (1960)898. J. W. Robinson, Anal. , 33 (1961)1226. T. Hadeishi and R. D. McLaughlin, Science, 174 (1971)404. J. W. Robinson, Atomic Absorption Spectroscopy, M. , 1975. G. F. Kirkbright, Atomic Absorption and Fluorescence Spectroscopy, M.
One obvious possibility is the analysis of two elements in a sample at the same time, thus halving analysis time. A less obvious attraction is the possibility of analysing via an internal standard. This is where a second element, either already present or added to the sample, is measured and ratioed to the analytical element. The Monochromator Channel A Monochromator Sample Beam Channel B Lamp Channel A Lamp Fig. 13. Dual channel optical arrangement. 34 analyte display is now independent of physical variations in atomiser characteristics.
Atomic Absorption Spectrometry by John Edward Cantle (Eds.)