By F. Heatley (auth.), Roger N. Ibbett (eds.)
ISBN-10: 9401049521
ISBN-13: 9789401049528
ISBN-10: 9401121508
ISBN-13: 9789401121507
R.N.IBBETT This e-book presents a resource of knowledge on all significant elements of NMR spectroscopy of man-made polymers. It represents a planned try and pull jointly the various strands of the topic in one finished quantity, designed to be readable at each clinical point. it really is meant that the e-book should be of use to nearly all of polymer scientists and NMR spec troscopists alike. Readers new to NMR will locate vast info in the ebook at the on hand strategies, permitting complete exploration of the various polymer technology purposes. Readers already verified inside of a department of NMR will locate the ebook an exceptional consultant to the sensible examine of polymers and the inter pretation of experimental info. Readers who've specialized in polymer NMR will locate the e-book a priceless dictionary of confirmed methodologies, in addition to a consultant to the very most up-to-date advancements within the topic. staff from the entire major branches of polymer NMR were invited to give a contribution. every one bankruptcy hence comprises info in relation to a parti cular investigative subject, indentified customarily at the foundation of approach. The e-book is loosely divided among answer and solid-state domain names, even supposing the various interconnections be certain that those domain names are components of an analogous continuum. uncomplicated rules are defined inside of every one bankruptcy, mixed with discussions of experimental concept and purposes. Examples of polymer investigations are lined generously and in lots of chapters there are discussions of the latest theoretical and experimental developments.
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Example text
10; the dependence of intensity on multiplicity and the variable is apparent. In practice, spectra deviate slightly from the ideal because of imperfect pulses and because of a range of values of Jew The APT sequence has the advantage that it is not necessary to have the ability to switch the 1 H RF power during the sequence from a high value required for broadband 1 H pulses to the lower value required for continuous 1 H decoupling. However, the DEPT sequence is more sensitive and more robust to variations in the value of Jew Also quaternary carbons do not appear in DEPT spectra.
23 (a) Comparison of (upper) the experimental and (lower) the calculated 220 MHz 1 H spectra of the CH 2 protons in free-radical poly(vinyl chloride) in chlorobenzene at 150°C. (b) Decomposition of the calculated spectrum into tetrad components. (Reprinted with permission from [59], as discussed in the text). in which vicinal coupling is absent. 19. e. a hexad. There are 32 hexads of which 20 are distinguishable. 4 The experimental observation of stereochemistry. It is worth pointing out some of the characteristics of the relationship between stereochemistry and NMR spectra which arise from the examples described.
01 v... i),~)NMR Spectroscopy of Polymers by F. Heatley (auth.), Roger N. Ibbett (eds.)
by Ronald
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